This paper is mainly concerned about how to purify the industrial products of the antioxidant d and bht , how to determine their purities , determining their purities and the purities need to be more than 99 % . in order to attain this objective , the recrystalizing method is used to purify antioxidant d and antioxidant bht . the methods of high performance liquid chromatography ( hplc ) is used to determine the chemical composition of the antioxidant d and bht , it is qualitative analysis 本论文是以防老剂d与bht工业品为主要原料制备防老剂d与bht标准物质,首先进行了防老剂d与bht的提纯和熔点的测定试验,并通过实验确定了防老剂d与bht重结晶提纯工艺;然后设计区域熔融装置,拟定操作规程和技术条件,通过用区域熔融法提纯重结晶后的防老剂d和bht产品满足标准物质的纯度要求。
区域: area; beat; reach; domain; p ...熔融: melt; melt-out; diatexis; si ...法: law区域熔融法成长: zone melting growth区域熔融: zone fusion; zone melting; zonemelting六次区域熔融: six zone pass区域熔融结晶: zone melting crystallization区域熔融提纯: zone melting purification区域精炼法 区域熔化 区域熔融: zonemelting无坩埚区域熔融: zone melting without crucible熔融法: fusion method; melting method; scorification高压熔融法: high pressure melting method熔融法生长: melt growth水热熔融法: hydrothermal melting method悬浮熔融法: levitation melting熔融法催干剂: fused drier碳酸钠熔融法: sodium carbonate fusion区域熔化: zone melting区域熔化法: zone melting区域熔炼: zonal melting; zone melting; zone refining; zoning区域熔炼法: zero recrystallization process; zone melting process区域熔炼炉: zone furnace区域熔炼器: zone refiner过氧化钠熔融法: vulcanized rubber - determination of total sulfur content - sodium peroxide fusion method磁悬区域熔炼: magnetic suspension zone-melting